Please use this identifier to cite or link to this item: https://hdl.handle.net/11147/2430
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dc.contributor.authorEanes, Ritchie C.-
dc.contributor.authorTek, Neslihan-
dc.contributor.authorKırsoy, Öyküm-
dc.contributor.authorFrary, Anne-
dc.contributor.authorDoğanlar, Sami-
dc.contributor.authorAlmeida, Adelia E.-
dc.date.accessioned2016-11-11T12:13:11Z
dc.date.available2016-11-11T12:13:11Z
dc.date.issued2008-01
dc.identifier.citationEanes, R. C., Tek, N., Kırsoy, Ö., Frary, A., Doğanlar, S., and Almeida, A. E. (2008). Development of practical HPLC methods for the separation and determination of eggplant steroidal glycoalkaloids and their aglycones. Journal of Liquid Chromatography and Related Technologies, 31(7), 984-1000. doi:10.1080/10826070801924741en_US
dc.identifier.issn1082-6076
dc.identifier.issn1082-6076-
dc.identifier.urihttp://doi.org/10.1080/10826070801924741
dc.identifier.urihttp://hdl.handle.net/11147/2430
dc.description.abstractA practical set of HPLC methods was developed for the separation and determination of the eggplant steroidal glycoalkaloids, solanine, chaconine, solasonine, solamargine, and their aglycones, solasodine and solanidine. A gradient method was initially developed, but proved to be neither robust nor practical. Three separate isocratic methods using acetonitrile and ammonium dihydrogen phosphate were developed and shown to be more repeatable, less subject to fluctuations in mobile phase composition, and less time consuming. The effect of adjusting buffer pH, column temperature, and buffer type (triethylammonium phosphate vs. ammonium dihydrogen phosphate) were evaluated. It was also discovered that, by addition of 10% methanol to the acetonitrile portion of the mobile phase, more control over the separations was possible. The use of methanol as a mobile phase entrainer greatly improved separations in some cases and its effectiveness was also dependent upon column temperature. Assessments of the method recovery, limit of detection, and limit of quantitation were made using extracts from S. melongena and S. linnaeanum.en_US
dc.description.sponsorshipTÜBİTAK, (Turkey) Project Number TBAG-2364 (103T139) and İzmir Institute of Technology Project Number 2004 IYTE 31en_US
dc.language.isoenen_US
dc.publisherTaylor and Francis Ltd.en_US
dc.relation.ispartofJournal of Liquid Chromatography and Related Technologiesen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectOrganic compoundsen_US
dc.subjectChaconineen_US
dc.subjectEggplanten_US
dc.subjectSolamargineen_US
dc.subjectSolanidineen_US
dc.subjectSteroidal glycoalkaloidsen_US
dc.titleDevelopment of practical HPLC methods for the separation and determination of eggplant steroidal glycoalkaloids and their aglyconesen_US
dc.typeArticleen_US
dc.authoridTR130616en_US
dc.authoridTR114295en_US
dc.authoridTR114553en_US
dc.authoridTR1977en_US
dc.contributor.departmentIzmir Institute of Technology. Chemistryen_US
dc.contributor.departmentIzmir Institute of Technology. Molecular Biology and Geneticsen_US
dc.identifier.volume31en_US
dc.identifier.issue7en_US
dc.identifier.startpage984en_US
dc.identifier.endpage1000en_US
dc.identifier.wosWOS:000253506700005
dc.identifier.scopusSCOPUS:2-s2.0-39749202177
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.identifier.doi10.1080/10826070801924741-
dc.relation.doi10.1080/10826070801924741en_US
dc.coverage.doi10.1080/10826070801924741en_US
item.languageiso639-1en-
item.fulltextWith Fulltext-
item.openairecristypehttp://purl.org/coar/resource_type/c_18cf-
item.cerifentitytypePublications-
item.grantfulltextopen-
item.openairetypeArticle-
crisitem.author.deptDepartment of Molecular Biology and Genetics-
crisitem.author.deptDepartment of Molecular Biology and Genetics-
Appears in Collections:Chemistry / Kimya
Molecular Biology and Genetics / Moleküler Biyoloji ve Genetik
Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection
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