Please use this identifier to cite or link to this item: https://hdl.handle.net/11147/12136
Full metadata record
DC FieldValueLanguage
dc.contributor.authorPişkin, Ceremen_US
dc.contributor.authorKaracasulu, Leventen_US
dc.contributor.authorIschia, Gloriaen_US
dc.contributor.authorBortolotti, Mauroen_US
dc.contributor.authorAhmetoğlu, Çekdar Vakıfen_US
dc.date.accessioned2022-07-06T09:36:41Z-
dc.date.available2022-07-06T09:36:41Z-
dc.date.issued2022-06-
dc.identifier.urihttps://doi.org/10.1111/jace.18349-
dc.identifier.urihttps://hdl.handle.net/11147/12136-
dc.description.abstractPotassium–sodium niobates (KxNa1−xNbO3, 0 < x < 1, KNN) were hydrothermally synthesized under varying alkaline ratios (K+/Na+), total hydroxide concentration, reaction temperature, and time. Compositional surveys were developed by using Rietveld analyses derived quantitative volume fractions. The data demonstrated that phase pure KNN synthesis can be achieved by reacting the niobium source with the hydroxide solution having 6 M total hydroxide concentration, cation ratio (K+/Na+) of above 6 at temperatures ≥200°C for 24 h. Dissolution–precipitation events through intermediate products including hexaniobates were postulated as a plausible formation mechanism. It was shown also that the single-phase KNN approaching the morphotropic phase boundary (MPB) could be obtained by further incorporation of sodium ions into the crystal via post-annealing at 800°C/2 h, following the hydrothermal synthesis.en_US
dc.language.isoenen_US
dc.publisherWileyen_US
dc.relation.ispartofJournal of the American Ceramic Societyen_US
dc.rightsinfo:eu-repo/semantics/embargoedAccessen_US
dc.subjectHydrothermal synthesisen_US
dc.subjectPotassium sodium niobateen_US
dc.subjectPowders materialsen_US
dc.titleHydrothermal synthesis of potassium–sodium niobate powdersen_US
dc.typeArticleen_US
dc.authorid0000-0002-0676-9369en_US
dc.authorid0000-0003-1222-4362-
dc.institutionauthorPişkin, Ceremen_US
dc.institutionauthorKaracasulu, Leventen_US
dc.institutionauthorAhmetoğlu, Çekdar Vakıfen_US
dc.departmentİzmir Institute of Technology. Materials Science and Engineeringen_US
dc.identifier.wosWOS:000747856800001en_US
dc.identifier.scopus2-s2.0-85123717466en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.identifier.doi10.1111/jace.18349-
dc.contributor.affiliation01. Izmir Institute of Technologyen_US
dc.contributor.affiliation01. Izmir Institute of Technologyen_US
dc.contributor.affiliationUniversity of Trentoen_US
dc.contributor.affiliationUniversity of Trentoen_US
dc.contributor.affiliation01. Izmir Institute of Technologyen_US
dc.relation.issn00027820en_US
dc.description.volume105en_US
dc.description.issue6en_US
dc.description.startpage3809-
dc.description.endpage3819-
dc.identifier.scopusqualityQ1-
item.fulltextWith Fulltext-
item.cerifentitytypePublications-
item.openairetypeArticle-
item.openairecristypehttp://purl.org/coar/resource_type/c_18cf-
item.grantfulltextembargo_20250701-
item.languageiso639-1en-
crisitem.author.dept01. Izmir Institute of Technology-
crisitem.author.dept01.01. Units Affiliated to the Rectorate-
crisitem.author.dept03.09. Department of Materials Science and Engineering-
Appears in Collections:Materials Science and Engineering / Malzeme Bilimi ve Mühendisliği
Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection
Files in This Item:
File Description SizeFormat 
Journal of the American Ceramic Society-2022.pdf
  Until 2025-07-01
Article1.94 MBAdobe PDFView/Open    Request a copy
Show simple item record



CORE Recommender

SCOPUSTM   
Citations

3
checked on Apr 5, 2024

WEB OF SCIENCETM
Citations

3
checked on Mar 23, 2024

Page view(s)

1,356
checked on May 20, 2024

Download(s)

2
checked on May 20, 2024

Google ScholarTM

Check




Altmetric


Items in GCRIS Repository are protected by copyright, with all rights reserved, unless otherwise indicated.