Synthesis and Characterization of Amido and Amido(monoalkylamido)nitrosyl-[tris(3,5 Complexes
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Date
1997
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Marcel Dekker Inc.
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Abstract
The chloro-amido complex [Mo{HB(3,5-Me2C3HN2)3}(NO)Cl(NH 2)] was prepared by treating [Mo{HB(3,5-Me2C3HN2)3}(NO)Cl 2] with an excess of ammonia. The monoalkylamido complexes [Mo{HB(3,5-Me2C3HN2)3}-(NO)(NH 2)(NHR)] (R = Me, Et, Pr-n and Bu-n) were obtained by the reaction of [Mo{HB(3,5-Me2C3HN2)3}(NO)Cl(NH 2)] with the appropriate primary amines. The IR and 1H NMR spectra of the new complexes were investigated.
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Synthesis(Chemistry), Molybdenum, Ammonia
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Citation
Topaloğlu, I., and McCleverty, J. A. (1997). Synthesis and characterization of amido and amido(monoalkylamido)nitrosyl-[tris(3,5-dimethylpyrazolyl)borato]molybdenum complexes. Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 27(8), 1205-1217. doi:10.1080/00945719708000258
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N/A
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1
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Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry
Volume
27
Issue
8
Start Page
1205
End Page
1217
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