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dc.contributor.advisorÇiftçioğlu, Muhsinen
dc.contributor.authorErdem, İlkeren
dc.date.accessioned2014-07-22T13:52:13Z
dc.date.available2014-07-22T13:52:13Z
dc.date.issued2002en
dc.identifier.urihttp://hdl.handle.net/11147/3716
dc.descriptionThesis (Master)--Izmir Institute of Technology, Biotechnology, Izmir, 2002en
dc.descriptionIncludes bibliographical references (pages 54-58)en
dc.descriptionText in English; Abstract: Turkish and Englishen
dc.descriptionxi, 58 leavesen
dc.description.abstractCeramic membranes possess desirable properties for industrial separation and concentration processes where extreme conditions of heat, pH, ionic strength are present. Ceramic composite membranes consisting of a support and a thin membrane layer with finer pores were prepared in this work. Ceramic supports were prepared from fine alumina and zirconia powders by dry-pressing and slipcasting.These supports were sintered in the 1100-1200°C temperature range.These supports were dip-coated with ceramic sols prepared from zirconium propoxide and aluminium isopropoxide for the preparation of thin layers with finer pores. Average particle sizes of these sols were measured as 3-7 nm for zirconia sol and 30-40 nm for alumina sol by laser scattering technique. The dipcoated membranes were calcined in the 500-600°C temperature range. The thermal characterization of membrane layers was determined with DTA/TGA. The microstructure of the ceramic composite membranes was investigated with SEM. The clean water permeability (CWP) of membranes was tested by using deionised water in a filtration set-up. Separation experiments were performed with bovine serum albumin (BSA, Stokes diameter: 7 nm) solution and whey to determine protein separation capacity of the composite membranes. The CWP of the dry pressed alumina supports heat treated at 1100°C was found to be higher than the permeability of the slip-cast zirconia supports heat treated at 1200°C. The protein retention of the slip-cast zirconia support was detected as 60% with UVVIS spectrophotmeter analysis (Abs. at 280nm). After the modification of the support with dip-coating protein retention of 96% was achieved. Then the composite membranes were used in whey protein concentration experiments. Whey, which is a complex biological liquid, containing proteins, carbohydrate, minerals, was fed to the membrane without any clarification process. The retention of whey proteins with dry-pressed alumina support modified with 1/4 diluted zirconia sol (calcination temperature: 500°C) was found to be 96% with a permeate flux of 40 Lm-2hour-1.en
dc.language.isoengen
dc.publisherIzmir Institute of Technologyen
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subject.lccTP248.25.M46 E73 2002en
dc.subject.lcshMembranes (Technology)en
dc.subject.lcshCeramic-matrix compositesen
dc.subject.lcshUltrafiltrationen
dc.titlePreparation of ultrafiltration/ microfiltration ceramic composite membranes for biotechnology applicationsen
dc.typemasterThesisen
dc.contributor.authorIDTR18512
dc.contributor.departmentIzmir Institute of Technology. Biotechnology and Bioengineeringen
dc.relation.publicationcategoryTezen_US


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